Thermal Conductivity & Thermoelectricity Analysis 

Measurements of thermal Conductivity coefficient and Thermoelectricity


InoTherm ® 
thermal conductivity meter
 The thermal conductivity coefficient is directly measured 

Accurate thermal conductivity coefficient values
errors for thermal conductivity coefficient not exceeding 
3% at k = 0.05 ÷ 1 W/m∙K, 
2% at k = 5 ÷ 150 W/m∙K, 
4% at k = 200 ÷ 500 W/m∙K. 

Versatile Thermal Conductivity meter

 

- Measure the Thermal Conductivity Coefficient of solids, liquids, powders, and pastes with InoTherm

 

- A sample to measure is the size of a bean!

 

- Measure the Seebeck Coefficient and the Thermal Conductivity Coefficient simultaneously with InoTherm-S  

 

Cost-efficient thermal conductivity measurements

 

 - Small samples 

Measured samples are discs with diameters from 8mm and heights from 0.5 mm or similar volumes of liquid or paste.

 - Artless sample preparation 

No polishing is required; the sample faces non-parallelism of up to 5 is allowed.

 - Short measuring time

7-minute measuring process with an instant thermal conductivity and thermoelectricity calculation.

Thermal conductivity meter electronic system stability

 

The thermal conductivity meter has a self-contained electronic system that operates the device and calculates the thermal conductivity coefficient and Seebeck coefficient. It does not depend on other hardware and software packages.

This is the thermal conductivity measurement process

The thermal conductivity coefficient of copper is measured directly. No unique settings, no additional values, no other nonsence. Just insert your sample and enjoy the results!

Thermal conductivity coefficient and thermal insulance of building materials

InoTherm-B 
A new thermal conductivity measuring device adapted for building materials.

Explicitly developed to measure low-conductive materials with a thermal conductivity coefficient between 0.002 and 10 W/m·K with the experimental error not exceeding 2%.

 

Reliable measurements of thermal insulance and thermal conductivity of composite walls.

 

Adjustable sample shapes and sizes. Round and rectangular samples with up to 100 mm dimensions can be used to measure the thermal conductivity of building materials. The instrument can be adjusted for larger samples at the customer’s request.

The thermal conductivity coefficient of hard and soft solids, powders, pastes, and gels can be measured.

 

Built-in sample thickness measurements with a precision of 0.01 mm. 

 

Controlled clumping force of up to 300 kg.

 

Self-contained electronic system. The instrument calculates the thermal conductivity coefficient immediately after the measurement procedure.

Measurements of thermal conductivity coefficients of building materials
Measurements of thermal Conductivity coefficient

Thermal conductivity phenomenon
 
 

Thermal conductivity refers to the ability of materials to transfer heat (e.g., thermal energy) from a body with higher thermal energy (e.g., with higher temperature) to a body with lower thermal energy (e.g., with lower temperature).  There are stationary and non-stationary thermal conductivity processes. The stationary thermal conductivity process occurs when the temperature difference remains constant. The non-stationary process is observed when the temperature difference changes with time.   

Different thermal conductivity measuring approaches are based on stationary and non-stationary (transient) thermal processes. The stationary process instruments measure the thermal conductivity directly, while the transient methods measure thermal diffusivity and then deduce the thermal conductivity.

Quantitatively, a material's capability to transfer heat is characterized by the thermal conductivity coefficient (k), which is the amount of heat passing through the homogeneous sample of unit length and unit area if the temperature difference is 1 K. In the International System of Units (SI), the thermal conductivity coefficient is expressed as W/(m·K).

 

During the stationary thermal conductivity process, the energy flux density is proportional to the temperature difference (see the picture). There: Q is the energy transferred through conductor thickness h during time t via the conductor area A. The equation shows that the value of k can be obtained given the temperature difference and the amount of heat transferred via the sample with known geometry.

 

 

 

InoTherm® is a unique, new-generation thermal conductivity measuring device for quick, direct measurements of thermal conductivity coefficient. Initially designed for solids, it can also measure the thermal properties of gels, liquids, and powders. 

 

The system measures the thermal energy that transfers from the heat source to the thermostat via the measured sample. The temperatures of the sample faces, the thermostat, and the surrounding air are precisely measured. 

The raw data are presented on the screen during measurement and automatically collected into a data file. After data processing, the file also contains the thermal conductivity coefficient and the calculated error margins. 

 

The instrument is factory-calibrated on standard samples and with all correction factors. It can be re-calibrated at the user site and by the user. The thermal conductivity measuring needs no other material parameters.

Heat flows through the sample while measuring the thermal conductivity coefficient
Electronic system for thermal conductivity meter
The foil samples to measure thermal conductivity coefficient

The InoTherm can now measure thermal conductivity of foils!

The thermal conductivity coefficients of 110 µm and 7,5 µm thickness of copper and aluminium foils were measured using the InoTherm thermal conductivity meter. The pieces in the picture were all we needed to measure the foils' thermal conductivity. The InoTherm results were 225 ± 8 W/mK for aluminium foil and 403 ± 15 W/mK for copper one. 

Why choose the InoTherm?

 - Direct measurements: The thermal conductivity of your material is measured in the most natural conditions of direct heat transfer.

 - Easy to use: 7 min to obtain the thermal conductivity, k,  value.

 - Data reliability and precision: The direct measurements of thermal conductivity have an error not exceeding 3% at k = 0.05 ÷ 1 W/m∙K, 2% at k = 5 ÷ 150 W/m∙K, and 4% at k = 200 ÷ 500 W/m∙K; the data acquired with InoTherm have been published in high rated materials science journals

- Undemanding sample preparation requirements: The sample for the thermal conductivity measurements should be a cylinder with a diameter starting from 7 mm and a thickness between 0.5 and 10 mm. Those are the smallest samples for direct heat flow measurements of thermal conductivity in the World! Only rough polishing of the solid sample faces is needed; up to 5 degrees of sample face non-parallelism is acceptable. The sample volume is just 0.1 ÷ 0.8 cm3, which is vital for expensive materials.

 - Versatility: The thermal conductivity coefficients of solids, liquids, gels, and powders can be measured. The Seebeck Coefficient and the Thermal Conductivity can be measured simultaneously with the InoTherm-S machine.

 - Digital system stability: The InoTherm is governed by a Raspberry Pi controller and thus does not depend on Windows updates. 

The InoTherm application areas:

 

 - Thermal protection systems

 

 - Thermoelectric power

 

 - Battery systems

 

 - Thermal insulation 

 

-  Building materials

 

- Polymer composites

 

 - Thermal conductive liquids

 

 - Thermal interface materials

 

 - Nanocomposites

 

 - Green Energy

 

 - Nuclear materials 

thermal conductivity measuring device
Thermal conductivity and Seebeck coefficient measuring device

Thermal conductivity measurement techniques comparison

thermal conductivity measurement instruments

* The method was designed for measuring of thermal diffusivity and thermal conductivity of homogeneous and isotropic materials only. A mixture of polymer and filler is neither isotropic nor homogeneous.

** Thermal conductivity is not directly measured but calculated, requiring knowledge of other material parameters

Thermal insulance and thermal conductivity measurements

Thermal insulance measurements

We can now measure thermal insulance (Y = ΔT/Φ): the temperature difference between two points for the unit heat flux (Φ = Q/tA) along them. Thermal insulance is especially relevant when describing the thermal resistance of the interface. It is also crucial to predict the efficient thermal conductivity of laminates. We found out that the thermal insulance of the Copper-Graphite interface is 6.5 K·mm2/W, while the same property for the 304 Stainless Steel-Graphite interface is 19 K·mm2/W. Currently, we cannot explain the difference. It is just a simple experimental fact acquired with our thermal conductivity measuring device InoTherm.

The value is essential for Li-ion battery packages and layered thermal protection systems. It can also be used for the thermal conductivity of thermoelectric composites.

The measurements were performed at a load of 30 MPa perpendicular to the contact surface. Our research is ongoing, and we invite you to follow us for more updates on thermal insulance. Fresh results will be posted soon here and on our LinkedIn page, keeping you at the forefront of this exciting field.

Thermal insulance and thermal resistance of the interface

Graphite – Graphite contact thermal insulance

We measured the graphite–graphite interface thermal insulance. Here is the dependence of the insulance (we denote it as Y) on the contact normal pressure. To compare, the Y value for a 3 mm thick bulk graphite plate (k = 160 W/mK) is shown as a punctured line. So, the contact resists the heat transfer stronger than a 3 mm thick plate up to the load of 10 MPa (approximately 100 kg/cm2). The results show the importance of load control while measuring the thermal conductivity of materials. Otherwise, the contact resistance will significantly affect the received thermal conductivity coefficient values.

How we send thermal conductivity instruments.

 Thermal conductivity is essential. The InoTherm system should safely go to our customer, so we put the device inside the soft box. 

We are now closing the box with the InoTherm. The thermal conductivity measuring core and the equipment's electronic system will be safe here. The customer will enjoy easy unpacking and installing the thermal conductivity apparatus.

thermal conductivity in the box
Thermal conductivity and Seebeck coefficient measuring device
packed thermal conductivity device

Our thermal conductivity coefficient measuring device, InoTherm, is ready for shipment to our customer. For accurate and dependable results in measuring composite material thermal conductivity, InoTherm is indispensable!

Thermal conductivity measuring device

History of the InoTherm

🔧 2018:
- First analogue thermal conductivity measuring device.

👨‍🔬 2021:
- Contact resistance is reduced, the experimental uncertainty is 10%. First paper is published.
 

👨‍💻 2022:
- System digitalisation. The experimental uncertainty is decreased to 5%. Paper in Journal of the European Ceramic Society is published.
 

🧙‍♂️ 2023:
- The experimental uncertainty is decreased to 2%.
- The InoTherm has a self-contained electronic system that operates the device and calculates the thermal conductivity coefficient.
- Industrial design.

Thermal conductivity measuring apparatus
Thermal conductivity coefficient of solids
Thermal conductivity measurements 2023

Please contact us to learn more about InoTherm

The thermal conductivity measuring instrument inner part

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